ABC26IN0172 · Lanthanides and Actinides

Subject: Inorganic Chemistry · Chapter: Lanthanides and Actinides · Topic: Magnetic Properties 4f · Exam: CSIR-NET 2015 · Marks: 2 · Difficulty: Medium

Consider the following statements for $\left(\mathrm{NH}_{4}\right)_{2}\left[\mathrm{Ce}\left(\mathrm{NO}_{3}\right)_{6}\right]$ (Z) (A) Coordination number of Ce is 12 (B) Z is paramagnetic (C) Z is an oxidising agent (D) Reaction of $\mathrm{Ph_3PO}$ with Z gives a complex having coordination number 10 for Ce. The correct statements are
(a)A, B and C
(b)B, A and D
(c)B, C and D
(d)A, C and D
Answer
Answer (as printed): D
Explanation
$(\mathrm{NH_4})_2[\mathrm{Ce(NO_3)_6}]$ (Z). (1) $\mathrm{NO_3^{-}}$ behaves as a bidentate ligand. Hence, C.N. $=12$. (2) $\mathrm{Ce^{4+}}$ has no unpaired electron, hence diamagnetic, not paramagnetic. (3) $\mathrm{Ce^{4+}}$ has a higher oxidation state, hence behaves as an oxidising agent. (4) $(\mathrm{NH_4})_2[\mathrm{Ce(NO_3)_6}]$ on reaction with $\mathrm{Ph_3PO}$ gives $[\mathrm{Ce(NO_3)_4(Ph_3PO)_2}]$ having C.N. $=10$. Hence, correct statement. $\mathrm{OPPh_3}$ = monodentate ligand; $\mathrm{NO_3}$ = bidentate.

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